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r-axis rapid ii curved imaging plate micro-diffractometer  (Rigaku Corporation)


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    Structured Review

    Rigaku Corporation r-axis rapid ii curved imaging plate micro-diffractometer
    R Axis Rapid Ii Curved Imaging Plate Micro Diffractometer, supplied by Rigaku Corporation, used in various techniques. Bioz Stars score: 90/100, based on 1 PubMed citations. ZERO BIAS - scores, article reviews, protocol conditions and more
    https://www.bioz.com/product/rapid+ii+curved+image+plate+diffractometer/xrd+patterns/10__5194_slash_ejm___37___169___2025-93-8-7
    Average 90 stars, based on 1 article reviews
    r-axis rapid ii curved imaging plate micro-diffractometer - by Bioz Stars, 2026-09
    90/100 stars

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    other:

    Article Title: Activation of Triphenylphosphine Oxide Mediated by Trivalent Organouranium Species
    Article Snippet: Crystal data Chemical formula C62H82B3N13O2U Mr 1311.86 Crystal system, space group Monoclinic, P21/c Temperature (K) 150 a, b, c (Å) 19.2372 (6), 12.3696 (5), 28.0124 (8) (°) 108.212 (2) V (Å 3 ) 6331.8 (4) Z 4 Radiation type Cu K (mm -1 ) 7.62 Crystal size (mm) 0.20 × 0.02 × 0.02 Data collection Diffractometer Rigaku Rapid II curved image plate diffractometer Absorption correction Multi-scan SCALEPACK (Otwinowski & Minor, 1997) Tmin, Tmax 0.777, 1.000 No. of measured, independent and observed [I > 2(I)] reflections 78440, 11904, 8970 Rint 0.049 (sin /)max (Å -1 ) 0.618 Refinement R[F 2 > 2(F 2 )], wR(F 2 ), S 0.044, 0.129, 1.12 No. of reflections 11904 No. of parameters 788 No. of restraints 174 H-atom treatment H-atom parameters constrained w=1/[σ 2 (Fo 2 )+(0.0738P) 2 +9.3126P] where P=(Fo 2 +2Fc 2 )/3 max, min (e Å -3 ) 2.67, -1.18 Refinement notes: A solvate THF molecule was refined as disordered.

    Article Title: Synthesis, kinetic studies, and atom transfer reactivity of [2Fe–2E] model compounds
    Article Snippet: The synthesis of [2Fe–2E] (E = S and Se) complexes supported by an N-alkyl,N’-aryl-β-diketiminate ligand is described.. The [2Fe–2S] model compound has an unusually long Fe⋯Fe distance, but the equivalent distance in the [2Fe–2Se] compound is comparable to those reported in the literature.. These model compounds display varying electron transfer capabilities, which were elucidated through electronic spectroscopy and electrochemical analysis.

    Article Title: Syntheses and Aromaticity Parameters of Hexahydroxypyrrocorphin, Porphotrilactones, and Their Oxidation State Intermediates.
    Article Snippet: Single crystal X-ray measurements for 12 were conducted on a Rigaku Rapid II curved image plate diffractometer with a Cu-Ka X-ray microsource (l = 1.54178 Å) with laterally graded multilayer (Goebel) mirrors for monochromatization.

    Article Title: Photophysical Properties of Pt(II) Polypyridines with Five- versus Six-Membered Chelate Rings: Trade-Offs in Angle Strain.
    Article Snippet: This report describes the synthesis and characterization of a series of eight [Pt(NNN)X] complexes where the tridentate NNN ligand is (2,2′-bipyrid-6-yl)(pyrid2-yl)sulfide (btp) or methyl(2,2′-bipyrid-6-yl)(pyrid-2-yl)amine (bmap) and X is OMe, Cl, phenylethynyl (C2Ph), or cyclohexylethynyl (C2Cy).. The expectation was that inserting a heteroatom into the backbone of 2,2′:6′,2′′-terpyridine (trpy) would expand the overall intraligand bite angle, introduce ILCT character into the excited states, and improve the photophysical properties.. Crystal structures of [Pt(bmap)C2Ph] + and [Pt(btp) Cl] reveal that atom insertion into the trpy backbone successfully expands the bite angle of the ligand by 8−10°.

    Article Title: Synthesis, characterization, DFT calculations, and reactivity study of a nitrido-bridged dimeric vanadium(iv) complex.
    Article Snippet: ion produces the aromatic tropylium cation, 135Hpt is one of the most hydridic hydrocarbons.. The G for this reaction, eq 2, is highly endergonic, + 72.5 kcal/mol.. As such, V2N2 is indicated to be very weakly hydridic.

    X-ray Diffraction:

    Article Title: Impact of Solid-State Form on the Disproportionation of Miconazole Mesylate.
    Article Snippet: .. Methods Single crystal X-ray diffraction Single crystal X-ray measurements were conducted on a Rigaku Rapid II curved image plate diffractometer with a Cu-Kα X-ray microsource (λ = 1.54178 Å) with a laterally graded multilayer (Goebel) mirror for monochromatization. .. Single crystals were mounted on Mitegen microloop mounts using a trace of mineral oil and cooled in-situ to 100(2) K for data collection.

    Article Title: Syntheses and Aromaticity Parameters of Hexahydroxypyrrocorphin, Porphotrilactones, and Their Oxidation State Intermediates.
    Article Snippet: .. Experimental Details to the X-ray Diffraction Analyses of 12 and 13 12 13 Crystal Data Chemical formula C41H4F20N4O6·2(CHCl3) C41H4F20N4O6·2(CHCl3) Mr C52H16F20N6O8Os·1.925(CHCl3) C62H24F20N8O12Os2·3.233(CH2Cl2) Crystal system, space group 1652.72 2107.92 Temperature (K) Monoclinic, P21/n Triclinic, P1# a, b, c (Å) 100 100 a, b, g (°#) 14.1435 (4), 21.6977 (6), 18.5339 (5) 13.6946 (4), 16.3712 (4), 17.2631 (6) V (Å3) 96.070 (2) 86.8724 (9), 71.2419 (12), 80.199 (2) Z 5655.8 (3) 3611.27 (19) F(000) 4 2 Dx (Mg m-3) 3206.6 2031.6 Radiation type 1.941 1.939 No. of reflections for cell measurement Cu Ka Mo Ka q range (°) for cell measurement 78677 39188 μ (mm-1) 4.1–72.3 1.8–30.7 Crystal shape 7.94 3.87 Colour Fragment Plate Crystal size (mm) Red Black Data Collection Diffractometer Rigaku Rapid II curved image plate diffractometer Nonius Kappa CCD diffractometer Radiation source microfocus X-ray tube fine focus X-ray tube Monochromator Laterally graded multilayer (Goebel) mirror Graphite Scan method w and phi scans Absorption correction Multi-scan, SCALEPACK (Otwinowski & Minor, 1997) S-42 Tmin, Tmax 0.642, 0.742 0.252, 0.497 No. of meas., indep. and obs. .. [I > 2s(I)] reflections 78677, 10923, 9117 39188, 18672, 14610 Rint 0.069 0.034 q values (°) qmax = 72.3, qmin = 4.1 qmax = 30.7, qmin = 1.8 (sin q/l)max (Å-1) 0.618 0.719 Range of h, k, l h = -17®17, k = -25®25, l = -22®22 h = -18®15, k = -20®23, l = -18®22 Refinement Refinement on F2 F2 R[F2 > 2s(F2)], wR(F2), S 0.064, 0.178, 1.11 0.040, 0.091, 1.08 No. of reflections 10923 18672 No. of parameters 1155 1203 No. of restraints 1350 462 H-atom treatment H-atom parameters constrained H-atom parameters constrained Weighting scheme w = 1/[s2(Fo2) + (0.0715P)2 + 48.8272P] where P = (Fo2 + 2Fc2)/3 w = 1/[s2(Fo2) + (0.011P)2 + 19.2033P] where P = (Fo2 + 2Fc2)/3 (D/s)max 0.001 0.002 Drmax, Drmin (e Å-3) 1.60, -3.05 1.76, -2.70 Extinction method SHELXL2014/7 (Sheldrick 2014, Fc*=kFc[1+0.001xFc2l3/sin(2q)]-1/4 SHELXL2014/7 (Sheldrick 2014, Fc*=kFc[1+0.001xFc2l3/sin(2q)]-1/4 Extinction coefficient 0.00045 (4) 0.00057 (5) CCDC # 2155695 2155696 Computer programs: CrystalClear-SM Expert 2.1 b32 (Rigaku, 2014), HKL-3000 (Otwinowski & Minor, 1997), SHELXS97 (Sheldrick, 2008), SHELXL2014/7 (Sheldrick, 2014), SHELXLE Rev714 (Hübschle et al., 2011).



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